INDEX PROPERTIES AND COMPACTION CHARACTERISTICS OF CEMENT-STABILIZED VERMI-REMEDIATED CRUDE OIL–CONTAMINATED BLACK COTTON SOIL FOR HIGHWAY SUBGRADE APPLICATIONS
Keywords:
Black cotton soil; vermi-remediation; cement stabilization; Atterberg limits; compaction; crude oil contamination; highway subgradeAbstract
Black cotton soil (BCS) contaminated with crude oil presents serious engineering and environmental challenges across oil-producing regions of Nigeria, particularly Borno State. Conventional stabilization of such soils without prior remediation is unsustainable and may not address hydrocarbon persistence. This study evaluates the index properties and compaction characteristics of vermi-remediated crude oil–contaminated black cotton soil stabilized with Ordinary Portland Cement (OPC) at 2%, 4%, 6%, and 8% by dry weight. Soil samples from Gamadadi, Borno State (10.320163°N, 11.5484146°E) were artificially contaminated at 8% crude oil by dry weight, bioremediated using Eisenia fetida earthworms over 30 days, and subsequently stabilized with cement. Laboratory tests—including Atterberg limits, specific gravity, particle size distribution (PSD), and proctor compaction under British Standard Light (BSL), West African Standard (WAS), and British Standard Heavy (BSH) efforts—were conducted in accordance with BS 1377 (1990). The vermi-remediation process achieved a total petroleum hydrocarbon (TPH) removal efficiency of 22.43%. The natural soil was classified as A-7-6 (19) (AASHTO) and CH (USCS), with a liquid limit (LL) of 57.8%, plasticity index (PI) of 29.15%, and specific gravity of 2.32. Cement addition progressively reduced LL from 55.0% to 48.0%, decreased PI from 25.37% to 13.68%, and reduced linear shrinkage from 16.43% to 12.86%. Specific gravity increased from 2.25 to 2.34 with cement content. Maximum dry density (MDD) exhibited a general decrease from 0–6% cement, then a slight recovery at 8%, across all compactive efforts (BSL: 1.63–1.62 Mg/m³; WAS: 1.77–1.74 Mg/m³; BSH: 1.85–1.83 Mg/m³). Optimum moisture content (OMC) increased from 0–6% cement and decreased slightly at 8%, with values consistently lower under higher compactive effort. Cement stabilization of vermi-remediated black cotton soil significantly improves index properties, though values remain above AASHTO base course thresholds. The treated soil demonstrates properties appropriate for use as subgrade and sub-base material, supporting sustainable reuse of petroleum-contaminated soils in highway construction.References
Abdulsalam A. B, (2024). Vermiremediation Of Crude Oil Contaminated Soil For Application As Highway Subgrade Material. An Unpublished MEng Dissertation Department of Civil Engineering, Nigerian Defence Academy Kaduna.
Adhikari, K., Roy, S., Rao, S., & Singh, A. K. (2022). Bioremediation of petroleum hydrocarbon-contaminated soil using earthworms: A review. *Environmental Science and Pollution Research*, 29(5), 6417–6432. https://doi.org/10.1007/s11356-021-17438-3
Ahmed, A., & Singh, B. (2025). Global perspectives on crude oil contamination and geotechnical impacts. *Geoenvironmental Engineering Reviews*, 12(1), 1–22.
Ahmed, F., Alam, S., & Khan, Z. (2024). Geotechnical behavior of crude oil–contaminated black cotton soil: A review of engineering challenges and remediation strategies. *Transportation Geotechnics*, 44, 101150. https://doi.org/10.1016/j.trgeo.2023.101150
Akinwumi, I. I., Okonkwo, C. A., & Adeyeri, J. B. (2014). Effects of crude oil contamination on the index properties, strength and permeability of laterite. *Journal of Environmental Science and Technology*, 7(5), 283–296. https://doi.org/10.3923/jest.2014.283.296
Almutairi, A. L. (2019). Bioremediation of petroleum hydrocarbon-contaminated soil using earthworms: Verification of quantitative and qualitative degradation. *Saudi Journal of Biological Sciences*, 26(7), 1397–1401. https://doi.org/10.1016/j.sjbs.2019.09.011
Almuaythir, S., Rahman, N. A., Adnan, A., & Al-Sharari, M. (2024). Geotechnical characterization of expansive black cotton soils from arid and semi-arid regions. *Engineering Geology*, 328, 107320. https://doi.org/10.1016/j.enggeo.2024.107320
Alvares, C. M., da Luz, M. A., & Siqueira, L. F. (2021). Solidification/stabilization of hydrocarbon-contaminated soils using cementitious binders: A review. *Journal of Hazardous Materials*, 405, 124221. https://doi.org/10.1016/j.jhazmat.2020.124221
Ameen, A. A., Yusuf, S. M., & Hassan, A. (2024). Compaction and strength behavior of cement-treated expansive soils under varying compactive efforts. *Geotechnical and Geological Engineering*, 42(3), 1551–1565. https://doi.org/10.1007/s10706-023-02676-4
Amnesty International. (2022). *Nigeria: Oil spills and human rights violations in the Niger Delta – 2018–2022 Report*. Amnesty International Publications.
Amu, O. O., Adetuberu, A. A., & Salami, O. T. (2022). Influence of crude oil contamination on stabilized black cotton soil properties for road construction. *International Journal of Civil Engineering and Technology*, 13(2), 44–57.
AASHTO. (2022). *Standard specifications for transportation materials and methods of sampling and testing* (43rd ed.). American Association of State Highway and Transportation Officials.
ASTM. (2023). *Annual book of ASTM standards: Soil and rock (I)* (Vol. 04.08). American Society for Testing and Materials.
Bada, B. S., Medupin, R. O., Salam, A. S., & Ukagwu, C. C. (2019). Determination of total petroleum hydrocarbon content in crude oil-polluted soil using gas chromatography-mass spectrometry. *Nigerian Journal of Pure and Applied Sciences*, 32(1), 3344–3352.
Behzad, A., & Abolfazl, E. (2021). Effect of cement and lime on Atterberg limits of expansive soils: A comparative study. *Arabian Journal of Geosciences*, 14, 1562. https://doi.org/10.1007/s12517-021-08196-6
BS 1377. (1990). *Methods of test for soils for civil engineering purposes*. British Standards Institution.
BS 1924. (1990). *Methods of test for stabilized materials for civil engineering purposes*. British Standards Institution.
BS EN 197-1. (2011). *Cement – Part 1: Composition, specifications and conformity criteria for common cements*. British Standards Institution.
Chachina, S. B., Voronkova, N. A., & Baklanova, O. N. (2016). Bioremediation of the petroleum and diesel-contaminated soils with earthworm Eisenia fetida. *Procedia Engineering*, 152, 122–133. https://doi.org/10.1016/j.proeng.2016.07.631
Chachina, S. B., Voronkova, N. A., & Baklanova, O. N. (2018). Bioremediation of heavily oil-contaminated soils using Dendrobaena veneta combined with bio-activator. *Procedia Engineering*, 206, 1539–1549.
Das, B. M., & Sobhan, K. (2023). *Principles of geotechnical engineering* (10th ed.). Cengage Learning.
Fadugba, O. G., Salami, A. T., & Osinubi, K. J. (2024). Compaction characteristics of cement-stabilized expansive soils under different compactive efforts: Implications for pavement design. *Road Materials and Pavement Design*, 25(2), 421–437. https://doi.org/10.1080/14680629.2023.2214501
Fatemeh, A., Hamid, S., & Mahdi, K. (2021). Effect of cement stabilization on Atterberg limits and engineering behavior of expansive clay soils. *Geotechnical and Geological Engineering*, 39, 3869–3882. https://doi.org/10.1007/s10706-021-01698-4
Federal Ministry of Works and Housing (FMWH). (2023). *General specifications for roads and bridges in Nigeria* (revised). Federal Republic of Nigeria.
Garba, L. S., & Yunana, D. A. (2023). Engineering properties of black cotton soils in northeastern Nigeria: A geotechnical characterization study. *Nigerian Journal of Engineering*, 30(1), 12–24.
Gertsen, A. A., Smirnov, A. V., & Kovalev, A. N. (2024). Impact of petroleum hydrocarbons on soil geomechanical properties: Experimental investigation. *Environmental Earth Sciences*, 83, 204. https://doi.org/10.1007/s12665-024-11452-5
Gong, X., Hu, Y., Gao, Y., & Wu, L. (2023). Enhancement of petroleum hydrocarbon degradation in soil by Eisenia fetida: A systematic review. *Science of the Total Environment*, 870, 162021. https://doi.org/10.1016/j.scitotenv.2023.162021
Goswami, M., Chakraborty, P., Mukherjee, K., Mitra, G., Bhattacharyya, P., Dey, S., & Tribedi, L. C. (2022). Bioaugmentation and biostimulation: The two key approaches in bioremediation of petroleum hydrocarbon contaminated soil. *FEMS Microbiology Letters*, 369(2), fnac027. https://doi.org/10.1093/femsle/fnac027
Head, K. H. (1994). *Manual of soil laboratory testing: Vol. 1. Soil classification and compaction tests* (2nd ed.). Pentech Press.
Huang, C., Guo, X., Lu, Y., Chen, X., & Wang, J. (2024). Earthworm–microbe interactions in petroleum hydrocarbon-contaminated soil: Mechanisms and applications in phytoremediation. *Journal of Hazardous Materials*, 462, 132752. https://doi.org/10.1016/j.jhazmat.2023.132752
Ingles, O. G., & Metcalf, J. B. (1972). *Soil stabilization: Principles and practice*. Butterworth-Heinemann.
Jalal, F. E., Xu, Y., Nasir, M. W., Jalal, M., & Iqbal, M. (2023). Geotechnical behavior of crude oil–contaminated soils: A state-of-the-art review. *Environmental Science and Pollution Research*, 30, 12344–12362. https://doi.org/10.1007/s11356-022-24219-3
Kamaruddin, S. A., Azimi, M. A., Hashim, R., Ariffin, E. H., & Yusoff, M. A. (2020). A review of cement stabilization on geotechnical properties of tropical soft soil. *Materials Today: Proceedings*, 31(2), A12–A25. https://doi.org/10.1016/j.matpr.2020.11.095
Moses, G. (2021). Geotechnical properties of black cotton soils from selected locations in Nigeria. *Journal of Engineering and Earth Sciences*, 15(2), 78–91.
NOSDRA. (2023). *Oil spill statistics in Nigeria: 2018–2022 annual report*. National Oil Spill Detection and Response Agency, Federal Republic of Nigeria.
NNPC. (2023). *Annual statistical bulletin* (19th ed.). Nigerian National Petroleum Company Limited.
Nigerian General Specifications for Roads and Bridges. (2016). *Volume II: Construction*. Federal Ministry of Works, Power and Housing.
Oluwatuyi, O. E., Ashaka, E. C., & Ojuri, O. O. (2023). Cement stabilization of crude oil–contaminated laterite for highway construction. *Transportation Geotechnics*, 38, 100916. https://doi.org/10.1016/j.trgeo.2022.100916
Osinubi, K. J., Eberemu, A. O., Gadzama, E. W., & Ijimdiya, T. S. (2022). Review of the use of microorganisms in geotechnical engineering applications. *SN Applied Sciences*, 4, 89. https://doi.org/10.1007/s42452-022-04974-3
Owagboriaye, F. O., Dedeke, G. A., Aladesida, A. A., Bamidele, J. A., & Owa, S. O. (2019). Reproductive performance, stress response and vermiremediation potential of earthworm Eisenia fetida (Savigny, 1826) in soil contaminated with glyphosate-based herbicide. *Applied Soil Ecology*, 143, 146–155. https://doi.org/10.1016/j.apsoil.2019.05.027
Oyediran, I. A., & Enya, J. (2021). Variation of specific gravity and other geotechnical properties with cement content in tropical expansive soils. *Geomechanics and Engineering*, 26(5), 431–441.
Sani J. E., Muhammad M. S, Victor I. M, Moses G. (2026a). Influence Of Coconut Shell Ash-Enhanced Filter Media in Electrokinetic Remediation (EKR) Treatment of Petroleum-Contaminated Soils. IRE Journals Volume 9 Issue 10 | ISSN: 2456-8880 DOI: https://doi.org/10.64388/IREV9I10-1717139
Sani J. E., Isah, I. K. Victor I. M, Moses G (2026b). Performance Evaluation of Vermi-Remediated Crude Oil Contaminated Soil on Compaction Characteristics When Stabilized with Cement Kiln Dust. IRE Journals Volume 9 Issue 11 |PP. 1797 – 1805. ISSN: 2456-8880 DOI: https://doi.org/10.64388/IREV9I11-1717773.
Sani J. E. Arome, A. Y. Musa Nasiru, Moses Ochu. B. O.O. (2026c). Strength Characteristics of Cement-Stabilized Vermi-Improved Crude Oil Contaminated Lateritic Soil under British Standard Light Compactive Effort for Highway Application. Journal of science technology and education 14(2), JUNE, 2026 E-ISSN: 3093-0898, PRINT ISSN: 2277-0011; Journal homepage: www.atbufstejoste.com
Rahman, M. A., Imteaz, M. A., Arulrajah, A., & Disfani, M. M. (2023). Suitability of black cotton soil for road construction: A review of engineering properties and stabilization methods. *Construction and Building Materials*, 370, 130634. https://doi.org/10.1016/j.conbuildmat.2023.130634
Sani, J. E. (2012). Cement stabilization of black cotton soil. *Nigerian Journal of Technology*, 31(2), 150–158.
Speight, J. G. (2014). *The chemistry and technology of petroleum* (5th ed.). CRC Press.
Subair, A., Ibrahim, S., & Bello, A. A. (2024). Effect of cement content and compactive effort on the mechanical properties of stabilized black cotton soil. *Geotechnical and Geological Engineering*, 42(4), 2183–2198. https://doi.org/10.1007/s10706-023-02801-3
Tyagi, B., Singh, A., Kumari, P., & Sharma, N. (2021). Bioremediation of petroleum hydrocarbon-contaminated soil: Current status and future directions. *Journal of Environmental Management*, 293, 112887. https://doi.org/10.1016/j.jenvman.2021.112887
Umar, M., Kassim, K. A., Ping, C. T. J., & Mung, S. (2025). Time-dependent strength development of cement-treated expansive soils: Role of curing age and cement content. *Soils and Foundations*, 65(1), 101209. https://doi.org/10.1016/j.sandf.2024.101209
Downloads
Published
Issue
Section
License
Copyright (c) 2026 ADVANCED JOURNAL OF ENGINEERING AND SCIENTIFIC APPLICATIONS

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.